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Easily Constructed Spectroelectrochemical Cell for Batch and Flow Injection Analyses

UNCP Author/Contributor (non-UNCP co-authors, if there are any, appear on document)
Dr.. Paul Flowers, Professor of Chemistry (Creator)
Institution
The University of North Carolina at Pembroke (UNCP )
Web Site: http://www.uncp.edu/academics/library

Abstract: The design and performance of an easily constructed spectroelectrochemical cell suitable for batch and flow injection measurements are described. The cell is fabricated from a commercially available 5 mm quartz cuvet and employs 60 ppi reticulated vitreous carbon as the working electrode, resulting in a reasonable compromise between optical sensitivity and thin layer electrochemical behavior. The spectroelectrochemical traits of the cell in both batch and flow modes were evaluated using aqueous ferricyanide and compare favorably to those reported previously for similar cells.

Additional Information

Publication
Analytical Chemistry, 2002, 74 (3)
Language: English
Date: 2002
Keywords
Spectroelectrochemistry, Microscale Analysis, Electrochemical Cell, Batch and Flow Injection Measurements